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Solution-State Nuclear Magnetic Resonance (NMR) Spectroscopy
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Nuclear magnetic resonance (NMR) spectroscopy is achieved by exciting an atom's quantum spin state and examining the energy released during its relaxation. This provides information on the identity and environment of the molecules present. Additionally, the longer relaxation time scale associated with NMR allows for various molecular dynamics and kinetics to be studied.
Capabilities
- ✓Compound identification
- ✓Molecular kinetics
- ✓Molecular dynamics
- ✓Molecular diffusion
- ✓Mixture analysis
- ✓High dynamic range digital console with two RF channels, SGU3 high dynamic range receiver, HPLNA high power low noise preamplifier, and 2G DigiLock™ direct RF digital lock
- ✓BLAH 300 watt 1H/19F transmitter and BLAX 500 watt 6-365 MHz BB transmitter
- ✓GRASPTM II gradient spectroscopy
- ✓SmartVT variable temperature control unit with BCU-II sample cooling to -50 ºC and NMR thermometer software
- ✓Oxford 600/51 magnet with TMC anti-vibration legs
- ✓TopSpin 3.5 pl2 software (CentOS Linux 5.11)
- ✓Bruker 5mm ultra-high sensitivity multinuclear Prodigy™ CryoProbe (liquids):Observation and decoupling of 1H, 19F and X-nuclei (frequency range 31P–15N)Z-axis gradient coil and ATMVariable temperature range -40°C to +80°C
- ✓Observation and decoupling of 1H, 19F and X-nuclei (frequency range 31P–15N)
- ✓Z-axis gradient coil and ATM
- ✓Variable temperature range -40°C to +80°C
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