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Nuclear magnetic resonance (NMR) spectroscopy is achieved by exciting an atom's quantum spin state and examining the energy released during its relaxation.β―This provides information on the identity and environment of the molecules present. Additionally, the longer relaxation time scale associated with NMR allows for various molecular dynamics and kinetics to be studied. Due to atomic spin state interactions with molecular electron orbitals, normal solid-state radio frequency absorbances tend to be broad and unanalyzable.Β Using magic angle spinning solid-state NMR spectroscopy, artificial "molecular tumbling" can be introduced, improving the resolution otherwise associated with solid-state NMR and creating analyzable spectra.
Capabilities
- βDrug polymorph studies
- βSolid materials analysis
- βSolid dynamic studies
- βInsoluble polymer studies
- βThree RF channels with waveform generators and openVnmrJ
- βVariable temperature capabilities
- βAutomated deuterium (2H) gradient shimming
- βPrimarily utilized for magic angle spinning (MAS) solid-state NMR spectroscopy
- βVarian 5mm AutoX DB probe:VT: -80 to +130C1H/19F, X (15N-31P), and 2H lockZ-axis pulsed field gradients and ATM
- βVT: -80 to +130C
- β1H/19F, X (15N-31P), and 2H lock
- βZ-axis pulsed field gradients and ATM
- βPhoenix 1.6 mm HXY probe for Solid-State NMR:VT: -125 to +125C1H/19F, X (31P-29Si), and Y (23Na-15N)Manual tune/matchCapable of spinning up to 40 kHz MAS
- βVT: -125 to +125C
- β1H/19F, X (31P-29Si), and Y (23Na-15N)
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